After Analyze, Method Validation is the pane that looks at the method and batch as a whole — curves, recoveries, and limit flags — not only one selected sample.

When to open it

Day-to-day single-peak work still lives on Results, chromatograms, and the calibration plot. Method Validation does not replace those views.

What you typically review

Area What to look for
Curves R² / fit against MinCurveR2; points cleared with Use; Origin / blank-offset intercept
Recovery RecPct, DevPct, RecFlag on known-dose bottles
Response / identity MinRsp / MaxRsp, MinQValue, qualifier counts, co-elution
Range Results above the top calibrator (AboveCurveMaximum) and overall PassFailFlag

Exact columns follow the method limits you configured — see Result limits & flags.

Layout

You can dock Method Validation like any other pane and save it in a .qtl layout. Layout Priority controls which saved layout wins when several presets compete — see Workspace and layouts.

Workflow

  1. Configure limits and CalGroups on the method (Method design, CalGroup & standard addition).
  2. Analyze.
  3. Open Method Validation and scan flags / recoveries.
  4. Clear bad cal points or fix doses / types, then Analyze again.
  5. Export reports when the validation picture is acceptable (Reports, import, and export).

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